Synthetic Procedures in Nucleic Acid Chemistry: Physical and physicochemical aids in characterization and in determination of structureW. Werner Zorbach, R. Stuart Tipson Interscience Publishers, 1968 - 674 pages |
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Page 39
... solution constant . Titration is performed with hydrochloric acid or potassium hydroxide ( 0.1 or 1.0 M ) . The potassium hydroxide must be entirely free from carbonate . Sodium hydroxide is unsuitable , because glass electrodes are ...
... solution constant . Titration is performed with hydrochloric acid or potassium hydroxide ( 0.1 or 1.0 M ) . The potassium hydroxide must be entirely free from carbonate . Sodium hydroxide is unsuitable , because glass electrodes are ...
Page 542
... solutions for detection are used with purines , pyrimidines , and their derivatives , the paper either being sprayed with the solution , or transported gently through a bath containing the solution . Many methods of detection are known ...
... solutions for detection are used with purines , pyrimidines , and their derivatives , the paper either being sprayed with the solution , or transported gently through a bath containing the solution . Many methods of detection are known ...
Page 615
... solution of dichlorodimethylsilane in benzene or carbon tetrachlo- ride is recommended . The column , thoroughly cleaned and degreased , is almost filled with the solution ; it is allowed to stand for some time , and then the solution ...
... solution of dichlorodimethylsilane in benzene or carbon tetrachlo- ride is recommended . The column , thoroughly cleaned and degreased , is almost filled with the solution ; it is allowed to stand for some time , and then the solution ...
Contents
Introduction | 4 |
Substituents that Create Acidic | 12 |
The Pyrimidine Nucleosides | 22 |
Copyright | |
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Common terms and phrases
5'-phosphate 9-methyl absorption Acta Crystallogr adenine adenosine Amer ammonium angle anomeric configuration anomeric proton aqueous assigned bands base bond carbon cation Chem chemical shift chromatography column compounds conformation crystal curve cytidine cytosine D. J. Brown deuterium doublet effect elution guanine Guanosine heterocyclic HOCH2 hydroxyl hypoxanthine imidazole infrared intensity ionization J. J. Fox mass spectra method methyl group methyl sulfoxide-d6 mixture molecule neutral species NH2 NH2 nitrogen atom nucleic acid nucleic acid components nucleo nucleosides Nucleosides and Nucleotides observed obtained p.m.r. spectroscopy p.m.r. spectrum Patterson map peak PH References phate phosphate pKa values positive Cotton-effect proton protons on C-2 purine purine nucleosides pyridine pyrimidine pyrimidine nucleosides R. K. Robins reflections resonance ring sample separation singlet solution solvent Spectra of Purines structure substituents Table technique Thiol thymine tion trimethylsilyl ultraviolet Ultraviolet Spectra uracil uridine wavelength Wavenumber рка